{"id":9423,"date":"2012-10-23T11:36:17","date_gmt":"2012-10-23T11:36:17","guid":{"rendered":"https:\/\/www.upjs.sk\/informacie\/vyskum\/inovacie-rozvoj-eu-problematika\/unikatne-pristroje\/laboratorium-strukturnej-analyzy\/"},"modified":"2022-09-12T20:45:31","modified_gmt":"2022-09-12T20:45:31","slug":"laboratorium-strukturnej-analyzy","status":"publish","type":"page","link":"https:\/\/www.upjs.sk\/informacie\/vyskum\/inovacie-rozvoj-eu-problematika\/unikatne-pristroje\/laboratorium-strukturnej-analyzy\/","title":{"rendered":"Laborat\u00f3rium \u0161trukt\u00farnej anal\u00fdzy"},"content":{"rendered":"
Laborat\u00f3rium \u0161trukt\u00farnej anal\u00fdzy Pr\u00edrodovedeckej fakulty UPJ\u0160 (L\u0160A) pod veden\u00edm prof. RNDr. Juraja \u010cern\u00e1ka, CSc.<\/a> je vybaven\u00e9 po\u010d\u00edta\u010dom riaden\u00fdm (obr. 1) \u0161pi\u010dkov\u00fdm monokry\u0161t\u00e1lov\u00fdm difraktometrom XCalibur (Oxford Instruments) s polohovo citliv\u00fdm detektorom (CCD area detector Sapphire 2) a\u00a0grafitov\u00fdm monochrom\u00e1torom (obr. 2). Existuj\u00faci z\u00e1kladn\u00fd pr\u00edstroj bol postupne dovybaven\u00fd chladi\u010dom kry\u0161t\u00e1lov Desktop Cooler (obr. 3), ktor\u00fd umo\u017e\u0148uje realizova\u0165 merania pri \u013eubovo\u013enej teplote v\u00a0teplotnom intervale 170 a\u017e 293 K\u00a0a\u00a0gener\u00e1torom Spellman DF60N3 z prostriedkov projektov\u00a0 \u0160F \u201eExtrem – Centrum pokro\u010dil\u00fdch fyzik\u00e1lnych \u0161t\u00fadi\u00ed materi\u00e1lov v extr\u00e9mnych podmienkach\u201c (ITMS 26220120005) a \u201eExtrem – Dobudovanie Centra pokro\u010dil\u00fdch fyzik\u00e1lnych \u0161t\u00fadi\u00ed materi\u00e1lov v extr\u00e9mnych podmienkach\u201c (ITMS 26220120047) v celkovej hodnote viac ako 77 tis. \u20ac.<\/p>\n Monokry\u0161t\u00e1lov\u00fd difraktometer XCalibur <\/strong>je zariadenie ur\u010den\u00e9 na zber difrak\u010dn\u00fdch d\u00e1t z\u00a0monokry\u0161t\u00e1lov. Na z\u00e1klade nameran\u00fdch d\u00e1t sa ur\u010duj\u00fa z\u00e1kladn\u00e9 kry\u0161talografick\u00e9 \u00fadaje o\u00a0sk\u00famanej l\u00e1tke (mrie\u017ekov\u00e9 parametre, priestorov\u00e1 grupa s\u00famernosti) a\u00a0n\u00e1sledn\u00fdm spracovan\u00edm \u00fadajov sa ur\u010d\u00ed trojrozmern\u00e1 kry\u0161t\u00e1lov\u00e1 \u0161trukt\u00fara sk\u00famanej l\u00e1tky, to je ak\u00fdmi chemick\u00fdmi v\u00e4zbami a\u00a0medzimolekulov\u00fdmi silami s\u00fa at\u00f3my posp\u00e1jan\u00e9 do molek\u00fal a\u00a0n\u00e1sledne do trojrozmernej priestorovej \u0161trukt\u00fary. Na z\u00edskanie kompletn\u00fdch d\u00e1t posta\u010duje ve\u013ekos\u0165 kry\u0161t\u00e1lu v\u00a0rozsahu od 0,1 do 0,5 mm.<\/p>\n Laborat\u00f3rium \u0161trukt\u00farnej anal\u00fdzy je lokalizovan\u00e9 v\u00a0priestoroch Katedry anorganickej ch\u00e9mie \u00dastavu chemick\u00fdch vied na Moyzesovej 11 na prvom poschod\u00ed. B\u00fdval\u00e9 nevyhovuj\u00face priestory boli zrekon\u0161truovan\u00e9 a\u00a0prestavan\u00e9 vr\u00e1tane vybavenia klimatiz\u00e1ciou v\u00a0celkovej hodnote takmer 10 tis. \u20ac, najm\u00e4 za podpory projektov APVV a\u00a0VEGA. \u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0<\/p>\n","protected":false},"excerpt":{"rendered":" Laborat\u00f3rium \u0161trukt\u00farnej anal\u00fdzy Pr\u00edrodovedeckej fakulty UPJ\u0160 (L\u0160A) pod veden\u00edm prof. RNDr. Juraja \u010cern\u00e1ka, CSc. je vybaven\u00e9 po\u010d\u00edta\u010dom riaden\u00fdm (obr. 1) \u0161pi\u010dkov\u00fdm monokry\u0161t\u00e1lov\u00fdm difraktometrom XCalibur (Oxford Instruments) s polohovo citliv\u00fdm detektorom (CCD area detector Sapphire 2) a\u00a0grafitov\u00fdm monochrom\u00e1torom (obr. 2). Existuj\u00faci z\u00e1kladn\u00fd pr\u00edstroj bol postupne dovybaven\u00fd chladi\u010dom kry\u0161t\u00e1lov Desktop Cooler (obr. 3), ktor\u00fd umo\u017e\u0148uje realizova\u0165 merania … \u010c\u00edta\u0165 \u010falej<\/a><\/p>\n","protected":false},"author":1,"featured_media":9426,"parent":3973,"menu_order":14,"comment_status":"closed","ping_status":"closed","template":"","meta":{"_acf_changed":false,"_editorskit_title_hidden":false,"_editorskit_reading_time":0,"_editorskit_is_block_options_detached":false,"_editorskit_block_options_position":"{}","footnotes":""},"class_list":["post-9423","page","type-page","status-publish","has-post-thumbnail","hentry"],"acf":{"acf_link_na_externy_obsah":""},"yoast_head":"\n
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