{"id":20293,"date":"2021-03-23T15:32:48","date_gmt":"2021-03-23T15:32:48","guid":{"rendered":"https:\/\/www.upjs.sk\/prirodovedecka-fakulta\/pracoviska\/ufv\/vv\/infr\/spolocne-laboratorium-tem\/"},"modified":"2022-11-13T21:31:09","modified_gmt":"2022-11-13T20:31:09","slug":"spolocne-laboratorium-tem","status":"publish","type":"cpt_pracoviska","link":"https:\/\/www.upjs.sk\/prirodovedecka-fakulta\/pracoviska\/ustavy-pf\/ufv\/vv\/infr\/spolocne-laboratorium-tem\/","title":{"rendered":"Spolo\u010dn\u00e9 laborat\u00f3rium TEM"},"content":{"rendered":"<h4 class=\"bordova\"><strong>Osoba zodpovedn\u00e1 za laborat\u00f3rium, kontakt, financovanie<\/strong><\/h4>\n<p>Spolo\u010dn\u00e9 laborat\u00f3rium transmisnej elektr\u00f3novej mikroskopie m\u00e1 \u0161tat\u00fat spolo\u010dn\u00e9ho laborat\u00f3ria so Slovenskou akad\u00e9miou vied, konkr\u00e9tne s \u00dastavom materi\u00e1lov\u00e9ho v\u00fdskum, experiment\u00e1lnej fyziky a geofyziky. Ved\u00facim laborat\u00f3ria je prof. RNDr. J\u00e1n Dusza, DrSc. (jdusza@imr.saske.sk) a jeho z\u00e1stupcom prof. RNDr. Pavol Sov\u00e1k, CSc (pavol.sovak@upjs.sk). Za hlavn\u00e9ho oper\u00e1tora bol menovan\u00fd Ing. Vladim\u00edr Girman, PhD (vladimir.girman@upjs.sk). Laborat\u00f3rium bolo vybudovan\u00e9 v r\u00e1mci rie\u0161enia projektu zo \u0161truktur\u00e1lnych fondov \u201eNanoCEXmat II &#8211; Budovanie infra\u0161trukt\u00fary Centra excelentnosti progres\u00edvnych materi\u00e1lov s nano a submikr\u00f3novou \u0161trukt\u00farou \u201d (EU ERDF European Regional Development Fund, Grant No. <strong>ITMS 26220120035<\/strong>).<br \/> \u00a0<\/p>\n<h4 class=\"bordova\"><strong>Umiestnenie laborat\u00f3ria<\/strong><\/h4>\n<p>Laborat\u00f3rium SLTEM je umiestnen\u00e9 v zrekon\u0161truovan\u00fdch priestoroch suter\u00e9nu \u00dastavu fyzik\u00e1lnych vied Pr\u00edrodovedeckej fakulty UPJ\u0160 v Ko\u0161iciach, Park Angelinum 9.<br \/> \u00a0<\/p>\n<h4 class=\"bordova\"><strong>Experiment\u00e1lne vybavenie laborat\u00f3ria<\/strong><\/h4>\n<p>V laborat\u00f3riu SLTEM je umiestnen\u00fd transmisn\u00fd elektr\u00f3nov\u00fd mikroskop <strong>JEOL JEM 2100F UHR<\/strong> v celkovej hodnote 832 tis. \u20ac (obr. 1). Mikroskop je ur\u010den\u00fd na \u0161t\u00fadium \u0161trukt\u00fary a sub\u0161trukt\u00fary tuh\u00fdch anorganick\u00fdch l\u00e1tok pomocou zv\u00e4zku elektr\u00f3nov a RTG \u017eiarenia.<br \/> Pracuje s ur\u00fdch\u013eovac\u00edm nap\u00e4t\u00edm v rozsahu od 80 do 200kV. Osvet\u013eovacia \u010das\u0165 je vybaven\u00e1 Schottkyho FEG kat\u00f3dou s extr\u00e9mne vysok\u00fdm v\u00fdkonom a trojstup\u0148ov\u00fdm kondenzorom. Zobrazovacia \u010das\u0165 pozost\u00e1va z dvojstup\u0148ovej objekt\u00edvovej \u010dasti, trojstu\u0148ovej intermedi\u00e1lnej a projektorovej \u010dasti. Kon\u0161truk\u010dne je laden\u00e1 na ultra vysok\u00e9 rozl\u00ed\u0161enie (0.19 nm) a maxim\u00e1lne zv\u00e4\u010d\u0161enie 1.5Mx. Koeficient sf\u00e9rickej a chromatickej vady hlavnej objekt\u00edvovej \u0161o\u0161ovky je 0.5, resp. 1.1 mm. Fokusovate\u013en\u00fd priemer zv\u00e4zku zodpoved\u00e1 hodnote spot size od 2 do 5 nm.<br \/> Podporou pre mikroskop je nieko\u013eko stup\u0148ov\u00e1 v\u00e1kuov\u00e1 s\u00fastava, z\u00e1lo\u017en\u00e9 zdroje s bat\u00e9riami, chladi\u010de s uzavret\u00fdm okruhom vody, klimatiz\u00e1cia laborat\u00f3ria a antistatick\u00e1 vodiv\u00e1 podlahovina.<br \/> \u00a0<\/p>\n<h4 class=\"bordova\"><strong>V\u00fdskumn\u00e9 mo\u017enosti<\/strong><\/h4>\n<p>Mikroskop predstavuje modern\u00fd n\u00e1stroj pre mikro a nanoanal\u00fdzy materi\u00e1lov. Poskytuje v\u0161etky metodiky zobrazenia konven\u010dnej transmisnej elektr\u00f3novej mikroskopie, tj. pozorovanie vo svetlom (BF) a tmavom poli (DF), centrovan\u00e9 tmav\u00e9 pole (CDF), dvojl\u00fa\u010dov\u00e9 ostvetlenie (WBDF), at\u010f.. V spojitosti s dr\u017eiakom pre n\u00e1klon prepar\u00e1tu v osiach X a Y umo\u017e\u0148uje pozorovanie \u0161trukt\u00far a\u017e na \u00farovni atom\u00e1rneho rozl\u00ed\u0161enia (HRTEM). Pre podrobnej\u0161ie \u0161trukt\u00farne alebo kry\u0161talografick\u00e9 anal\u00fdzy v TEM re\u017eime je mo\u017en\u00e9 pou\u017ei\u0165 techniky elektr\u00f3novej difrakcie (SAED, NBD, CBED). V\u00fdsledky je mo\u017en\u00e9 podpori\u0165 anal\u00fdzou chemick\u00e9ho zlo\u017eenia EDS technikou pomocou RTG \u017eiarenia. Analyz\u00e1tor pracuje s energiov\u00fdm rozl\u00ed\u0161en\u00edm 129eV a pokr\u00fdva oblas\u0165 detegovate\u013en\u00fdch prvkov od uhl\u00edka po ur\u00e1n.<br \/> Roz\u0161\u00edrenie analytick\u00fdch mo\u017enost\u00ed je zabezpe\u010den\u00e9 vybaven\u00edm mikroskopu skenovac\u00edmi cievkami a STEM detektormi pre svetl\u00e9 pole a tmav\u00e9 pole (ADF a HAADF), kde je mo\u017en\u00e9 vyu\u017e\u00edva\u0165 techniku zobrazenia rozlo\u017eenia at\u00f3mov (Z-contrast). Sn\u00edmkovanie pozorovan\u00fdch \u0161trukt\u00far je vyrie\u0161en\u00e9 prostredn\u00edctvom digit\u00e1lnej kamery.<br \/> \u00a0<\/p>\n<h4 class=\"bordova\"><strong>Fotogal\u00e9ria<\/strong><\/h4>\n","protected":false},"author":1,"featured_media":15067,"parent":20272,"menu_order":18,"template":"","meta":{"_editorskit_title_hidden":false,"_editorskit_reading_time":0,"_editorskit_is_block_options_detached":false,"_editorskit_block_options_position":"{}"},"categories":[],"tags":[],"tax_aktuality":[],"acf":{"acf_link_na_externy_obsah":""},"yoast_head":"<!-- This site is optimized with the Yoast SEO plugin v22.7 - https:\/\/yoast.com\/wordpress\/plugins\/seo\/ -->\n<title>Spolo\u010dn\u00e9 laborat\u00f3rium TEM - Pr\u00edrodovedeck\u00e1 fakulta | UPJ\u0160<\/title>\n<meta name=\"robots\" content=\"index, follow, max-snippet:-1, max-image-preview:large, max-video-preview:-1\" \/>\n<link rel=\"canonical\" href=\"https:\/\/www.upjs.sk\/prirodovedecka-fakulta\/pracoviska\/ustavy-pf\/ufv\/vv\/infr\/spolocne-laboratorium-tem\/\" \/>\n<meta property=\"og:locale\" content=\"sk_SK\" \/>\n<meta property=\"og:type\" content=\"article\" \/>\n<meta property=\"og:title\" content=\"Spolo\u010dn\u00e9 laborat\u00f3rium TEM - Pr\u00edrodovedeck\u00e1 fakulta | UPJ\u0160\" \/>\n<meta property=\"og:description\" content=\"Osoba zodpovedn\u00e1 za laborat\u00f3rium, kontakt, financovanie Spolo\u010dn\u00e9 laborat\u00f3rium transmisnej elektr\u00f3novej mikroskopie m\u00e1 \u0161tat\u00fat spolo\u010dn\u00e9ho laborat\u00f3ria so Slovenskou akad\u00e9miou vied, konkr\u00e9tne s \u00dastavom materi\u00e1lov\u00e9ho v\u00fdskum, experiment\u00e1lnej fyziky a geofyziky. 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